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9—TGA-DTA curves for PGE-551435 Lots 3 and 4 hygroscopicity samples. Changes in water content over the RH conditions are consistent with a channel type hydrate. PGE-551435 Conclusions Sequential use of light microscopy, x-ray powder diffraction, and TGA-DTA provided rapid confirmation that the four samples represented two different solid state forms. TGA-DTA data and the hygroscopicity challenge identified the form of Lots 1 and 2 as an anhydrate. The TGADTA data identified the form of Lots 3 and 4 as a channel type hydrate.

Bigalow Kern,1 Wendy J. Collins,1 R. ,2 and Nancy L. 3 Use of a TG/DTA/Raman System to Monitor Dehydration and Phase Conversions ABSTRACT: Use of a TG/DTA/Raman system enabled real time collection of Raman spectra during the dehydration of Risedronate, the active pharmaceutical ingredient in the osteoporosis drug Actonel. Raman spectra collected during the dehydration of this material show a crystal lattice adjustment below the boiling point of water facilitating interpretation of the TG/DTA thermal profile.

Raman Spectroscopy, Vol. 29, 1998, pp. 97–102. , and Chang, H. , Applied Physics, Vol. 86, 1999, p. 6779. BIGALOW KERN ET AL. , Reviews in Analytical Chemistry, Vol. 20, No. 3, 2001, pp. 207–238. [9] Chang, H. and Huang, P. , Analytical Chemistry, Vol. 69, 1997, pp. 1485–1491. [10] Huang, P. , Thermochimica Acta, Vol. 297, 1997, pp. 85–92. , Thermochimica Acta, Vol. 371, 2001, pp. 127–135. , Materials Chemistry and Physics, Vol. 58, 1999, pp.

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A manual of time and motion study by J W Hendry


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